Fe/SBA-15: Characterization and its application to a heterogeneous solar photo-Fenton process in order to decolorize and mineralize an azo dye

TONCÓN-LEAL, C.F.; SAPAG, K.; DOS SANTOS, A.J.; MARTÍNEZ-HUITLE, C.A.; ARROYO-GÓMEZ, J.J.; MORENO, M.S.

Materials Letters: X

Elsevier

Año: 2019 vol. 5

2590-1508

Fe/SBA-15 catalyst with different iron (Fe)loads(6% and 10% wt.) was synthesized via incipient wetness impregnation. The potential photocatalytic properties were tested using solar radiation, as a novel catalyst in heterogeneous Fenton approach to degrade Methyl Orangeazo dye. A partial pore blocking of the substrate by Fe nanoparticles was detected and the main form of Fe present was Fe2O3. When the Fe(10%)/SBA-15 catalyst was used for heterogeneous solar photo-Fenton reaction, total discoloration of the effluent was achieved in 90 min, and 89% of COD was removed in 240 min. Short-chain linear carboxylic acids were followed over time, as well as inorganic ions