INVESTIGADORES
ECHEVERRIA Gustavo Alberto
artículos
Título:
Synthesis, crystal and molecular structure of methyl ((4-acetamidophenyl)sulfonyl) carbamate, precursor of Herbicide asulam
Autor/es:
P. CASTILLO; A. GOMEZ; H. MARQUEZ; A. M. PLUTIN; M. MORALES; R. POMES; Y. RODRIGUEZ; G. PUNTE; G. ECHEVERRÍA
Revista:
CNIC serie ciencias químicas
Referencias:
Año: 2002 vol. 33 p. 77 - 81
ISSN:
0254-0525
Resumen:
X-Ray diffraction and IR, NMR 1H and 13C spectroscopic data have been used to characterize methyl ((4-acetamidophenyl) sulfonyl)carbamate, precursor of the herbicide ASULAM. The title compound was synthesized by a conventional procedure and its crystal and molecular structure have been determined from single crystal X-Ray diffraction data. Crystals are monoclinic, space group P21/n; a=8.681(4), b=8.174(3), c=17.583(3)Å, ß=92.40(1)º, Z=4. The molecular packing shows a bidimensional hydrogen bond network.
