Síntesis de un composite de nanopartículas soportadas en grafeno químicamente reducido

C, COSIO CASTAÑEDA; RICARDO MARTÍNEZ GARCÍA; LEANDRO M. SOCOLOVSKY

Villahermosa, Tabasco

Congreso; VII Congreso Nacional de Cristalografía; 2014

Sociedad Mexicana de Cristalografía. Instituto de Física, UNAM

Novel gamma-Fe2O3@APTES@rGO composites are successfully synthesized by using graphene oxide and silanized maghemite nanoparticles. Graphene oxide and maghemite were obtained by Hummers and Massart methods, respectively. The silanization process was done to functionalize maghemite surface with a controllable quantity of amino groups. Then, by adding aqueous graphene oxide suspension, the bonding between graphene oxide and silanized maghemite nanoparticles was done in refluxing conditions. Afterwards, chemical reduced graphene oxide reaction was realized by addition of hydrazine solution. The characterization of -Fe2O3@APTES@rGO composites was studied by X-ray Diffraction, Fourier Transformed Infrared Spectroscopy, thermogravimetric analysis and scanning electron microscopy.