CCT ROSARIO   20442
CENTRO CIENTIFICO TECNOLOGICO CONICET - ROSARIO
Centro Científico Tecnológico - CCT
congresos y reuniones científicas
Título:
Microstructural Evolution of a Heterogeneous Austenitic Stainless Steel Processed by Equal Channel Angular Sheet Extrusion (ECASE)
Autor/es:
TARTALINI, VANINA; MUÑOZ, JAIRO; BOLMARO, RAÚL; RISSO, PABLO; ÁVALOS, MARTINA
Lugar:
CABA
Reunión:
Congreso; XV Congreso Internacional CIASEM; 2019
Institución organizadora:
Sociedad Argentina de Microscopía
Resumen:
Stainless steels stand out for their excellent properties such as corrosion resistance, high temperature resistance  and  good  formability  among  others  [1?4].  From  a  mechanical  point  of  view,  austenitic  stainless steels are materials that attract attention due to their wide mechanical strength range that can be achieved mainly due to the deformation induced phase transformation phenomenon, from austenite fcc to martensite bcc [5?7]. In this study, an austenitic stainless steel (≤0.03C; 18?20Cr; 69.9?74% Fe; ≤2Mn; 8?12Ni; ≤0.045P; ≤1Si; ≤0.03S (wt%)) in the form of Sheet (20 mm wide and 5 mm thick) was processed by 1 ECASE pass at room temperature using a matrix with an inner channel angle of Ф = 150 ° (see Figure 1). Before processing the material, a heat treatment was carried out at 850 ° C for 2 h and subsequent water quenching. The microstructure characterization was carried out by electron backscattered diffraction (EBSD). Samples were cut from the transversal direction (TD) plane and prepared by mechanical polishing until colloidal silica suspension with a particle size of 0.02μm. The data  was  processed  with  TSL  OIM  7.3b  software.  The  software  processing  parameters  were: Maximum misorientation threshold of 5 ° to calculate grain size and a cleaning subroutine to remove unindexed points using the grain dilation method taking into account a minimum size of 4 points. After ECASE processing, it was found that greater deformations were introduced around the sheet edges, while the middle area remained less affected by the deformation. The greater deformations at the edges caused  a  greater  transformation  from  austenite  to  martensite,  resulting  in  a  heterogeneous  structure  along the sheet thickness, as shown in Figure 1.Tensile tests revealed that after the deformation process, the material increased its yield strength almost 3 times from 200MPa in its initial state to 600MPa. In Figure 2a it can be seen that tensile tests in different areas of the sheet thickness revealed a heterogeneous behavior with tougher and less ductile areas (greater amount of bcc martensite) and other more ductile but softer areas (greater amount of austenite). The main objective of this research is the study of mechanical and microstructural properties of a heterogeneous structure in an austenitic stainless steel deformed by ECASE maintaining a good strength-ductility ratio. The heterogeneous structure obtained consists mainly of a more pronounced phase  change  in  the  sheet  edges  vicinity  than  the  middle  zone,  as  well  as  a  greater  Geometrically  Necessary Dislocations (GND) density at the edges than the middle zone (see Figure 2b). For this reason,  through  mechanical  tests  and  microstructural  characterization,  the  ductility  and  strength  contributions of each of these areas to the heterogeneous material was studied.