INVESTIGADORES
SCAFFARDI Lucia Beatriz
artículos
Título:
VISIBLE AND NEAR INFRARED BACKSCATTERING SPECTROSCOPY FOR CHARACTERIZATION OF SPHERICAL MICROPARTICLES
Autor/es:
L. B. SCAFFARDI; F. VIDELA; D. C. SCHINCA
Revista:
APPLIED OPTICS
Editorial:
Optical Society of America (OSA)
Referencias:
Lugar: Washington; Año: 2007 vol. 46 p. 67 - 75
ISSN:
0003-6935
Resumen:
Scattering is a useful tool for the determination of particle size in solution. Particularly, spectroscopic
analysis of backscattering renders the possibility of a simplified experimental setup and a direct data
processing using Mie theory. We show that a simple technique based on near-infrared (NIR) backscattering
spectroscopy together with the development of the corresponding algorithm based in Fourier
transform (FT) and Mie theory, are a powerful tool for sizing microparticles in the range from 8 to 60 m
diameter. There are three wavelength intervals in the NIR, within which different diameter ranges were
analyzed. In each one of them, FT yields a coarse diameter value with an uncertainty dependent on the
wavelength range. A more accurate value is obtained by further applying cross correlation between
experimental and theoretical spectra. This latter step reduces the uncertainty in diameter determination
between 30% and 40%, depending on wavelength interval and particle diameter. These results extend
previous information on visible backscattering spectroscopy applied to sizing microparticles in the range
between 1 and 24 m of diameter. This technique may the basis for the construction of a portable and
practical instrument.
practical instrument.
previous information on visible backscattering spectroscopy applied to sizing microparticles in the range
between 1 and 24 m of diameter. This technique may the basis for the construction of a portable and
practical instrument.
practical instrument.
diameter. There are three wavelength intervals in the NIR, within which different diameter ranges were
analyzed. In each one of them, FT yields a coarse diameter value with an uncertainty dependent on the
wavelength range. A more accurate value is obtained by further applying cross correlation between
experimental and theoretical spectra. This latter step reduces the uncertainty in diameter determination
between 30% and 40%, depending on wavelength interval and particle diameter. These results extend
previous information on visible backscattering spectroscopy applied to sizing microparticles in the range
between 1 and 24 m of diameter. This technique may the basis for the construction of a portable and
practical instrument.
practical instrument.
previous information on visible backscattering spectroscopy applied to sizing microparticles in the range
between 1 and 24 m of diameter. This technique may the basis for the construction of a portable and
practical instrument.
practical instrument.
m
diameter. There are three wavelength intervals in the NIR, within which different diameter ranges were
analyzed. In each one of them, FT yields a coarse diameter value with an uncertainty dependent on the
wavelength range. A more accurate value is obtained by further applying cross correlation between
experimental and theoretical spectra. This latter step reduces the uncertainty in diameter determination
between 30% and 40%, depending on wavelength interval and particle diameter. These results extend
previous information on visible backscattering spectroscopy applied to sizing microparticles in the range
between 1 and 24 m of diameter. This technique may the basis for the construction of a portable and
practical instrument.
practical instrument.
previous information on visible backscattering spectroscopy applied to sizing microparticles in the range
between 1 and 24 m of diameter. This technique may the basis for the construction of a portable and
practical instrument.
practical instrument.
% and 40%, depending on wavelength interval and particle diameter. These results extend
previous information on visible backscattering spectroscopy applied to sizing microparticles in the range
between 1 and 24 m of diameter. This technique may the basis for the construction of a portable and
practical instrument.
practical instrument.
m of diameter. This technique may the basis for the construction of a portable and
practical instrument.